
New TopShim run:

version = topshim 2.0.0
date = 2024-07-09
time = 10:47:12.559
command = topshim 

FINE SHIMMING

Parameters:

probe = Z168772_0022
solvent = CDCl3
shim nucleus = 2H
nucleus optimised for = 13C
o1p (from lock) = 7.24 ppm

Results:


1D Shimming:
shim changes: 
Z2	-2

duration = 27 sec
completed with failure
finished Tue Jul  9 10:47:38 2024


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New TopShim run:

version = topshim 2.0.0
date = 2024-07-09
time = 10:52:19.350
command = topshim 

FINE SHIMMING

Parameters:

probe = Z168772_0022
solvent = CDCl3
shim nucleus = 2H
nucleus optimised for = 13C
o1p (from lock) = 7.24 ppm

Results:


1D Shimming:
Iteration  1: FWHM Before= 0.5 Hz, Target= 0.3 Hz, After= 0.4 Hz
Iteration  2: FWHM Before= 0.4 Hz, Target= 0.4 Hz, After= 0.4 Hz
Iteration  3: FWHM Before= 0.4 Hz, Target= 0.4 Hz, After= 0.5 Hz
Iteration  4: FWHM Before= 0.5 Hz, Target= 0.5 Hz
Shim succeeded

Lineshape quality factor (1D spectrum, spinning) = 0.534

shim changes: 
Z	-26
Z2	+8
Z3	+56
Z4	-118
Z5	-75

duration = 2 min 55 sec
completed successfully
finished Tue Jul  9 10:55:13 2024


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New TopShim run:

version = topshim 2.0.0
date = 2024-07-09
time = 10:55:15.030
command = topshim  tunea tune

TUNE

Parameters:

probe = Z168772_0022
solvent = CDCl3

Results:


Performing tune after shimming
tune lock level increase = 1.0

shim changes: 
Z	-9
X	+2
XZ	+57
Y	+1

duration = 2 min 20 sec
completed successfully
finished Tue Jul  9 10:57:33 2024


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